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Single halsa, Halsafjorden


    Compounding of well-dispersed cellulose nanocomposites based on biodegradable polymers is challenging and commonly requires separate processes for wood fiber fibrillation into cellulose nanofibrils CNFfollowed by compounding.

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    Here, nanostructured biocomposites based on poly caprolactone PCL and holocellulose wood fibers HC were melt compounded in a single step. The grafting was performed by two different methods: the commonly used bulk method and a new approach using acetic acid AcOH as the reaction solvent to swell the fiber structure during grafting.

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    Remarkably, AcOH as a swelling solvent resulted in high density of grafts inside the nanostructure and throughout the volume of the HC wood cellulose fibers. As a consequence, more pronounced defibrillation of fibers into CNF during compounding as well as more uniform CNF dispersion in the thermoplastic PCL matrix was observed.

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    In contrast, fibers grafted under bulk conditions showed little grafting and weak reinforcement effects. The results show a close connection between the single halsa structure and final material properties.

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